Showing posts with label Energy. Show all posts
Showing posts with label Energy. Show all posts

Edible Oil Refinery Plant - Chemical Refining

Thursday, February 23, 2012

What is Oil Refinery and Edible Oil Refinery?

When talking about refinery, we need to be able to differentiate and identify an oil refinery from the edible oil refinery. Basically, the oil refinery (or petroleum refinery) is an industrial process plant where crude oil (from crude petroleum) is processed and refined into more useful petroleum products, such as gasoline, diesel fuel, asphalt base, heating oil, kerosene, and liquefied petroleum gas. This is the type of refinery mentioned in the 13 Days: Pythagoras Conspiracy Novel. An edible oil plant in the other hand, is almost similar to the earlier refinery accept it processes edible oil and involves the removal of fatty acid and a few more unwanted impurities. The edible oils are obtained from the likes of palm oil, soya bean oil, canola oil, corn oil, rape seed oil and others. In other words, the oil refinery process oil that cannot be consumed by human being while the edible oil refinery process oil that is edible (can be consumed by human beings).

I have no direct involvement in the oil refinery. However, I was a process engineer in an edible refinery plant before for quite some time. I had a really good taste of experience working in the refinery plant before. I strongly believe that if a chemical engineering student or a new chemical engineer wants to gain experience, he or she should work in a refinery. This is mainly because they will learn and apply all that they have learn in chemical engineering.

Edible Oil Refinery

Edible oil originates from crude oil such as crude palm oil (CPO), crude soya bean oil (CSBO), crude rape seed oil (CRSO), crude coconut oil (CCO) and so on. Edible oils have very high content of free fatty acids (FFA) and needs to be refined before using as cooking oil. However, the refinery process isn't only limited to remove FFA, it also removes the undesired components such as moisture, color and odour which may trigger negative impact on the final taste, odour and appearance of the oil product. The resultant oil is thinner without fatty acids, colorless and odorless.

It is imperative to note that the edible oil refinery can be divided into 2 primary types namely, chemical refining and physical refining. This time, I'll explain about the chemical refining plant.

Chemical Refining Plant

Chemical refining plant involve neutralization of crude oil by removing fatty acids. This is always referred to as chemical refining or sometimes Neutralizing process and its plant referred as Neutralizing Plant (NP). In this process the oil is neutralized in the neutralizer to remove the fatty acids by mixing with caustic soda (sodium hydroxide). Oil is heated up to roughly 60oC by and oil is stirred by stirrer. The fatty acids are settled at the bottom as alkali soaps which is called soapstock from where it is taken out into soap tank .

Typical Neutralizing Plant. Image credited to Oiltek Sdn Bhd, a Malaysian company that manufactures edible oil equipments. Click on the photo to enlarge it.

Removal of impurities and color

Neutralized oil is passed through the second vessel called bleacher where color of oil is removed by bleaching process with the help of chemicals such as carbon black and bleaching clay. Oil is usually heated up to 110oC. Stirring is also carried on. Bleaching process is done under vacuum. Bleached oil then goes to filtration process where bleaching clay and chemicals are removed and cleaned.

Removal of unpleasant smell

Bleached oil is then passed through deodorizer where oil is heated above 110C and then live steam clean is used to the oil from the bottom steam nozzles. The temperature of oil is raised up to 200 to 220C through thermic fluid coils. Entire process is done under high vacuum. Thus smell is removed from the oil in the deodorizer. Then it goes to cooler where cold water circulating coils take away heat and oil is cooled.

Final Filtration

Final filtration is performed after cooling down the oil. This operation is carried out in a micro filter closet or filter bag/filter cartridge which makes the final edible oil termed as refined edible oil. This final filtration process is designed for more effective filtration and best quality of final refined edible oil. There are certain refineries that adopted Hazard Analysis Critical Control Point (HACCP) to completely ensure that the oil is free and safe to be consumed.

This is a typical physical refinery plant. The image is also credited to Oiltek. Click the image to enlarge it.

In the next post, I'll describe more about the Physical Refinery. This is where I gained the most of my hands on chemical engineering experiences. This is where I learned more about important unit operations such as heat exchanger, cooling tower, deodoriser, pack coloumn etc.



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IEM Technical Visit to Mechmar Boiler

Friday, January 20, 2012

Last November I joined a group of Institution Engineers Malaysia (IEM) members for a technical visit trip to Mechmar Boiler in Pasir Gudang, Johor, Malaysia. This was the first time I visited a boiler manufacturer company. Honestly I was thrilled to learn and explore how a boiler is made and what the factory looks like. I mean the production plant site. In total there were about 20-30 engineers from IEM. The program started at 9.30 am up to 12.30 pm.


Some information about Mechmar Corporation (Malaysia) Berhad

Mechmar Boiler was established over 30 years ago. Currently, Mechmar Boiler is the leading industrial boiler and pressure vessel manufacturer within the Asian Pacific region.

With a core emphasis on superior engineering and strict manufacturing quality standards, Mechmar continually strives and meets the ever increasing expectations of today’s customers for reliable heat, power or steam generation at an economical investment cost.

Mechmar wide product range serves to meet the heat, steam or power needs of our customers regardless of their industry and location. Their products are the result of years of continuous and rigorous detailed engineering and dedication to providing quality in our manufacture and in our service to our customers.

The headquartered of Mechmar is in Kuala Lumpur, Malaysia. Mechmar’s engineering team reinforces their commitment to their customers by providing sound engineering input with attention to detail. With two world class manufacturing and fabrication facilities in South East Asia both of which are ISO9001 certified by Lloyds, we meet this commitment with speed and at competitive prices. (Information taken from Mechmar official website).

Products manufactured by Mechmar

Here are the list of products manufactured by Mechmar Corporation (Malaysia) Berhad:

Oil/Gas-Fired Boiler
  • Titan HT
  • Titan AS
  • Titan MB
Solid Fuel-Fired Boilers
  • Titan MCC
  • Titan MCH
  • Titan BD
  • Titan MTH
-Heat Recovery Boiler
-Various Custom Made Boilers
-Reconditioned boilers

For more comprehensive list of products, please click here.

The factory administrator of Mechmar Boiler gave us some explanation on the history and business of the company.

A nice pen as souvenir for the IEM delegates. Luckily they provided a free pen because I forgot to bring my own pen.

This is the view in the production facility of Mechmar Boiler
One of the oil/gas fired boiler nearly completed

That's me with some nice background in the Mechmar Boiler facility

Taking a group photo together in the boiler manufacturing plant




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My Ph.D Progress so far... Oct 2011 Updates

Tuesday, October 18, 2011

I'm now in my 5th semester and I must admit that I'm very worried with my own performance as a Ph.D student. I have basically 8 months more to complete my studies (I was given 3 years for a my full time Ph.D). Otherwise I will have to extend my study to another semester.

I am now midway in my experiments. I am also preparing several technical papers to be published in index journals. It's really not easy. The mood and motivation are always against me. Let's see today's example...

I tried to work on my technical paper draft in my office room. After several minutes I felt sleepy (I did not sleep late at night). Then, I experienced some headache. Both of this elements (sleepy + headache) makes a perfect combination to demotivate me from pursuing my work. I tried to fight the negativity. I relaxed for 2-3 minutes. Then, I thought myself...maybe I should do other work that still can contribute towards my study. I then decided to learn a new optimization method from youtube since I am going to include them in my study. So, I decided to stop working on the technical paper draft for a while and studied this new optimization method. It works... I felt energized to learn a new stuff. This is indeed a good technique which I personally discovered (maybe this is not new to you guys). I have the option of perhaps give up, rest, sleep, relax, chit-chat with my friends, drink some coffee, watch some movie in my laptop but instead I decided to work on something else which still contributes towards accomplishing and perfecting my thesis. I'm really glad to do that.

At the same time, to keep up my spirit and assure continuous momentum, I changed my desktop wall paper. It has a message that I should complete my study in the allocated time. This constantly reminds me that I have an unsettle business to complete (the Ph.D off course!!!). This is the final major hurdle that I need to conquer after the other 2 big projects which is to be a professional engineer and chartered engineer, all within a space of 3 years. Fuhhh.... it's really tough but I'm glad I managed to complete the other two.

Enough rambling for now. I'm going to continue with my work. Need to work on something... If you have any motivational quote for me, I really welcome and appreciate them very much. Thanks in advance.

p/s- The photo above shows the Thermal Gravimetric Analysis (TGA) equipment with its PC. The PC is very old. It still uses the 3.5" floppy disc. Although it is old, it is still very useful and important for me because it provide one part of my catalyst analysis. The TGA is still in good shape as it is regularly maintained.


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Power Failure in Our Industry!

Thursday, May 26, 2011

Once upon a time in the Chemical Reaction Engineering Research Laboratory


On a sweet Thursday afternoon (today) when I just started my experiment, a sudden power failure occurred without warning. I was actually in the toilet when the power cut off took place. My wife called and asked, "Do you have electricity there in the lab?". I answered, "We have power here in the lab and I just started my experiment". Then 2 lab assistants walk out from the polymer lab (which is next to the reaction engineering lab) and informed me that the power failure just happened. I was surprised.

Immediately I ran into the lab and discovered that the lab black out. Oh my God!!! This is not good. It's not really about my experiment. It's the Gas Chromatography (GC) which I'm more worried about. The GC is such an important equipment for me and the rest of the students as we use it to identify and quantify our products from the reactor. The GC is very sensitive and frequent power cut-off can jeopardize the equipment and interrupt our research activities. Repairing the GC cost huge amount of money and with limited research budget, we need to do everything to avoid the GC from malfunctioning.

After about 15 to 20 minutes the electrical power resumed. Thank God. I switched it on. I then checked the GC and its PC hoping that nothing will go wrong. When the power failure occurred just now, the oven temperature (of the GC) was 250oC. The standard operating procedure to switch off the GC is when the oven temperature is below 40oC. Sudden GC shut down is not recommended at all. It is strictly a big NO. Luckily the GC works well and nothing seems to be wrong. I restarted my experiment and completed it 3 hours later.

Power Failure in the Plant

The incident reminded me on the power failure that once in a while also occurred in the physical refinery plant I worked in several years ago. Such unavoidable power cut-off from the Electricity Company will firstly trigger chaos within the control room and the entire plant. The supervisor, shift leader and plant operators have to act fast to close all main valves manually from various sections. The flow, temperature and pressure from numerous unit operation equipment such as Niagara filter (filter leaves), deodoriser, packed column, heat exchanger need to be controlled until power resumed. The huge 3000 tonnes per day plant can only be minimally controlled via the PLC which was temporarily powered with UPS (uninterupted power supply) - which provided a few minutes power back up.

Secondly, the power cut off will result in substantial lost and I have to assess and make report about it. Even a milisecond power failure will result in vacuum drop in the plant in result to oil rejection (due to quality off-spec). That also will cost massive lost to the company.

What can we do?

As for my case, in the lab... nothing much can be done. I rest my faith to the God. It's good to install UPS for the GC. If UPS is the answer, then we must have 4 UPS unit in the lab as there are all together 3 GC's and 1 GCMS. However, having UPS alone will not entirely protect this expansive machines. For me, the power company (electricity supplier) must be responsible in providing smooth and reliable power for us (the customers). They should pay all the damage and losses that hit us. Maybe this does not sound like an engineer's solution...

Other option?

A more interesting option is to create and manage our own power system...but can we do it with our resources? I'm referring to solar, wind and frequency (Tesla) energy. I would love to develop one of this power sources AFTER I complete my study. I'll try and do it at my home first... :)


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Image #1 credited to: http://www.wkow.com/Global/story.asp?S=14691294&clienttype=printable
Image #2 credited to:
http://www.msnbc.msn.com/id/42761336/ns/us_news-life/t/refinery-warnings-way-life-texas-city/

My Ph.D study so far...

Tuesday, May 24, 2011

I'm now in my 4th semester of my Ph.D studies. I will be lying if I say that doing Ph.D is easy. It's not as easy as that. I told my wife few months ago that preparing the project report for my Institution Engineers Malaysia (IEM) interview (to be a professional engineer) was tougher than doing my Ph.D. I'm wrong!!! Maybe that time, I was not really focus on my Ph.D. But now, as I'm more focus with my studies, I am well aware that completing this study is not as easy as it seems to be. It is so tough. Ask anybody who successfully completed their Ph.D... Nobody says it is easy.

Suddenly I felt time is very limited. I'm beginning to feel the pressure. I have more or less one year to complete my studies. I need to start working on my experiments. My experimental rig is fine and I believe it will be ok as I already tested it several times. The only concern for me is the quartz reactor that is brittle in nature. I need to keep sufficient stock of it. In addition, I also need to ensure my other equipments and consumables have spare as well. When talking about the experimentation work, the Gas Chromatography (GC) should also be in perfect condition for me and my Iranian colleague (Maryam) to analyze our products. The GC is the basically the heart of the study besides the rig reactor and process. I'm going to start my experimental work tomorrow officially and I hope everything will be fine... (Need to pray a lot!!!) OK ...enough about the experimental work.

Journal Paper... This is another thing hunting my back and consuming a huge chunk of my time. I have a draft prepared and submitted to 2 reputed publishers only to see on both occasions it got rejected for funny reasons (the first one) and out of scope reason (the second one). I admit that I felt miserable being rejected just like that. Well... I need to bounce back and fight to improve my draft paper and then send it again to other journal.

Thermodynamic modeling... Yeah...not only experimental work, I also need to work on the thermodynamic modeling of my catalytic reaction. This is quite interesting but at the same time it is my weakest part. I'm slowly working on this section and I hope I can complete this study in the next 2 months... (also, I need to pray to God a lot on this). I'm receiving some help from Maryam on this. She has been helping me when I got confuse and lost.

There are certainly a lot more to share about my research journey as a Ph.D student. I think I should reserve the rest for future sharing. For the time being, I just need to focus on my study for a while. Wish me luck... :)

Before ending... I would like to thank my other half of her undivided support for me. It is good to have a partner who is also in the same chemical engineering field. She understood what I'm doing and at the same time provided me precious input and ideas.

Also, my other colleague in the lab... All of you are great...haha...especially Emm2020...who has been next door to me in the lab...Let's finish this together!!!

p/s: Sorry if this post is not of any benefit to you guys. I just need to vent off some tense in me.



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Have you downloaded my free "Choosing Alternative Fuel" Ebook? If not, then please download it here. It's Free and on top of getting the free ebook, you'll get eCourse on Alternative Fuel. It's a good and easy way to add more valuable information to yourself.

 
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